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SYNTHESIS AND CHARACTERIZATION OF WATER-SOLUBLE CdSe NANOPARTICLES CAPPED BY AOT

SYNTHESIS AND CHARACTERIZATION OF WATER-SOLUBLE CdSe NANOPARTICLES CAPPED BY AOT
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摘要 Water-soluble CdSe nanoparticles were synthesized using AOT (sodium bis(2-ethylehexyl)-sulfosuccinate) as stabilizer, cadmium acetate and NazSeSO3 as precursors in aqueous phase. The influence of some key factors, such as reaction time, temperature, concentration and molar ratio of precursors on the optical properties of CdSe nanoparticles was systematically investigated through UV-Vis and PL spectra. Powder X-ray diffraction (XRD) was used to characterize the crystalline structure of synthesized CdSe nanoparticles. As-prepared CdSe nanoparticles exhibit an apparent quantum confinement effect and typical hexagonal wurtzite structures. Finally, the optimal experimental conditions were obtained. Water-soluble CdSe nanoparticles were synthesized using AOT (sodium bis(2-ethylehexyl)-sulfosuccinate) as stabilizer, cadmium acetate and NazSeSO3 as precursors in aqueous phase. The influence of some key factors, such as reaction time, temperature, concentration and molar ratio of precursors on the optical properties of CdSe nanoparticles was systematically investigated through UV-Vis and PL spectra. Powder X-ray diffraction (XRD) was used to characterize the crystalline structure of synthesized CdSe nanoparticles. As-prepared CdSe nanoparticles exhibit an apparent quantum confinement effect and typical hexagonal wurtzite structures. Finally, the optimal experimental conditions were obtained.
出处 《Chinese Journal of Polymer Science》 SCIE CAS CSCD 2013年第9期1284-1289,共6页 高分子科学(英文版)
基金 supported by the Research Program of Liaoning Scientific Department (No. 05L302200644)
关键词 AOT CDSE NANOPARTICLES Aqueous phase. AOT CdSe Nanoparticles Aqueous phase.
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