摘要
通过核磁共振技术对从马蹄香中分离得到的马兜铃内酰胺IV进行了结构解析,第一次报道了该化合物的碳谱数据,并通过二维核磁共振(HSQC,HMBC)对其碳和氢信号进行了全归属,更正了文献[6,7]中H-2和H-5信号的归属错误.
The structure of aristololactam IV isolated from Sarurna henryi Oliv. was elucidated via NMR. The ,3 C NMR data and complete assigment of the 1H and 13 C chemical shifts of the compound by 2D NMR (HSQC, HMBC) was firstly obtained, and the assignments of H-2 and H-5 of the compound were also corrected.
出处
《波谱学杂志》
CAS
CSCD
北大核心
2013年第3期424-429,共6页
Chinese Journal of Magnetic Resonance
基金
国家林业公益性行业科研专项资助项目(200904004)