摘要
The as-cast and as-extruded Mg-9Li, Mg-9Li-0.3Ce alloys were respectively prepared through a simple alloying process and hot extrusion. The microstructures of these alloys were investigated by optical microscope (OM), scanning electron microscope (SEM), X-ray diffractometer (XRD) and energy dispersive spectrometer (EDS). The results indicate that Ce addition produces a strong grain refining effect in Mg-9Li alloy. The grain size of the as-extruded alloy reduces abruptly from 88.2 μm to 10.5 μm when the addition of Ce is 0.36%. Mg12Ce is verified and exists inside the grains or at the grain boundaries, thus possibly pins up grain boundaries and restrains the grain growth.
通过合金化和热挤压制备铸态及挤压态的Mg-9Li和Mg-9Li-0.3Ce合金,通过光学显微镜和扫描电镜观察结合能谱分析以及XRD分析对这一系列合金的微观组织进行研究。结果表明:Ce的添加对Mg-9Li合金有很好的晶粒细化效果,当Ce的添加量达到0.36%时,挤压态合金的尺寸从未添加的88.2μm减小至10.5μm,Mg12Ce存在于晶粒内或晶界处,因此认为Mg12Ce可能聚集在晶界处从而阻碍晶粒的长大。
基金
Project(2007CB613706)supported by the National Basic Research Program of China
Project(2009AA03Z507)supported by the National High-tech Program of China
Projects(2010CSTC-HDLS,CSTC2010AA4048)supported by Chongqing Science and Technology Commission,China