摘要
介绍了标题化合物的合成方法。以2,3-二氯吡啶为起始原料,经甲氧基取代、甲氧基水解、碘代和氯代反应合成了目标化合物,并经MS和1H NMR对其结构进行了表征。本合成路线原料易得、操作简便,适合于工业化生产。反应总收率51%。
In the paper, we introduced a approach to synthetize the title compound, was realized and manufactured from 2,3-dichloropyridine via four steps. Its structure was verified by MS and 1H NMR. This synthetic route has the advantages of convenient operation and mild reaction conditions. The total product yield was 51%. This program is suitable for industrial production.
出处
《广东化工》
CAS
2013年第17期230-230,共1页
Guangdong Chemical Industry
基金
贵州省中药现代化项目
合同编号:黔科合中药字[2010]5022号
贵州省教育厅自然科学课题
合同编号:黔教合KY字[2012]044号贵州省高层次人才科研条件特助经费项目
合同编号:TZJF-2010年-055号
