摘要
目的:对梅四膏质量标准进行研究,以便更好地控制内部质量。方法:对方中大黄、黄柏进行薄层色谱鉴别,对栀子中的栀子苷采用高效液相色谱法进行含量测定。结果:薄层色谱方法专属性好;栀子苷在0.24～3.00ug范围内线性关系良好,r=0.9996,平均回收率为98.72%,RSD为0.45%。结论:上述方法操作简单,重复性好,可作为质量控制依据。
Purpose：To develop the quality control of Meisi paste.Method：Rhubarb and Cortex Phellodendri in the prescription were identified by TLC.The content of Gardenia jasminoides were determined by HPLC.Result ：The calibration curve of geniposide was at the range of 0.24 to 3.00μg（r=0.9996）,and the recovery was 98.72 %and RSD was 0.45 %.Conclusion：The method has the advantages of simple operation,high repeatability and can be used for the quality control of Meisi paste.
出处
《内蒙古中医药》
2013年第26期33-34,共2页
Inner Mongolia Journal of Traditional Chinese Medicine
