摘要
本文采用煅烧的方法制备了Ag-掺杂的石墨型氮化碳(Ag/g-C3N4)材料。通过考查银与三聚氰胺的质量比,最终以6.25%作为最佳掺杂银量来制备此材料。同时本文也报道了该材料的光致发光(PL)行为,该行为对微量的Cu2+的检测具有较好的选择性,其检测限可达1nmol·L-1。可见,我们制备的这种材料为微量的Cu2+的检测提供了一个简单而方便的方法。
In this paper, considering the ratio of Ag and melamine, Ag-doped graphite-like carbon nitride (Ag/g-C3 N4 )material was finally prepared by calcining with 6. 25% the optimum doping ~.mount of Ag. The photoluminescence(PL) behavior of this material was studied,which demostrates that it is selective for the detection of trace amount of Cu^2+ , and the limit of detection was I nM. Thus,the as-prepared material provides a simple and convenient method for the detection of trace amount of Cu^2+.
出处
《化学研究与应用》
CAS
CSCD
北大核心
2013年第11期1470-1474,共5页
Chemical Research and Application
关键词
AG
g-C3N4
光致发光
Ag-doped graphite carbon nitride
photoluminescence