摘要
戊二酸酐和薄荷醇在4-二甲氨基吡啶(DMAP)的催化作用下,以甲苯为溶剂,合成新型清凉剂戊二酸单薄荷酯,收率为79.1%.产物的结构通过红外光谱、核磁共振光谱和质谱进行了表征.
The coolant agent monomenthyl glutarate was synthesized by a direct reaction glutaric anhydride with DMAP as the catalyst in toluene, and the yield can be up to 80%. The was characterized by IR, NMR and MS spectra, and monomenthyl glutarate was confirmed. between structure menthol and of compound
出处
《河南科学》
2013年第10期1607-1609,共3页
Henan Science