摘要
在微波辐射条件下采用双烧杯装置,首次合成了10种芳氧乙酸,产物结构经IR,1H NMR及元素分析进行了表征。实验表明,该法具有操作安全简便、反应时间短、易纯化及环境友好等优点,是一种有效合成芳氧乙酸的方法。
Ten aryloxyacetic acids were prepared firstly with double beaker device, using microwave heating methodology. Their chemical structures were confirmed by means of IR, 1 H NMR and elemental analysis. The results suggest that this method is an effective method of synthesis of aryloxy acetic acids with the advantages of safe and convenient operation, short reaction time, easy purification and environmental friendly, and so on.
出处
《贵州大学学报（自然科学版）》
2013年第5期19-21,26,共4页
Journal of Guizhou University:Natural Sciences
基金
国家自然科学基金(29571013)
甘肃省青年科技基金计划(1107RJYP047)
甘肃省自然科学基金(ZS021A25006Z)
甘肃省环保基金(GH200216)
甘肃民族师范学院的院长基金项目(10-04)
关键词
微波辐射
芳氧乙酸
合成
microwave irradiation
aryloxy acetic acids
synthesis
