期刊文献+

甲基环氧氯丙烷合成方法研究 被引量:3

Synthesis of 3\|chloro\|2\|methylpropene oxide
下载PDF
导出
摘要 以2甲基3氯丙烯为原料,在原有类似物的基础上,设计了两种合成路线,成功地合成出了甲基环氧氯丙烷.对两种合成方法进行优化选择,得出简便可行、反应时间短、产率高的合成方案. Chloro\|2\|methylpropene oxide has been prepared from 3\|chloro\|2\|methylpropene through two different synthesis methods. One has been proved, as compared with the other one, not only to be simle and convenient but also to have a shorter reaction time and a higher yield. So an effective way to synthesize the monomer was provided.
出处 《首都师范大学学报(自然科学版)》 1999年第4期40-43,共4页 Journal of Capital Normal University:Natural Science Edition
关键词 甲基环氧氯丙烷 聚合物单体 环氧树脂 合成方法 chloro\|2\|methyproperne oxide, monomer of polymer,epoxy resin.
  • 相关文献

参考文献1

共引文献4

同被引文献16

  • 1成卫国,王祥生,李钢,郭新闻.TS-1/尿素/过氧化氢体系中的丙烯环氧化反应(英文)[J].催化学报,2004,25(7):513-514. 被引量:6
  • 2江秀明,谢洪良.环氧稀释剂十二烷基缩水甘油醚的合成[J].热固性树脂,2004,19(6):18-19. 被引量:17
  • 3殷跃广,陈晓昀,米镇涛.TS-1催化H_2O_2与甲基氯丙烯环氧化[J].化学工业与工程,2006,23(1):21-24. 被引量:1
  • 4尹文华,贾文静,吴璧耀.环硫-环氧活性稀释剂的合成与性能研究[J].化工新型材料,2005,33(12):69-72. 被引量:3
  • 5Kitano Tomoyuki, Kikuzono Yasuo. The Epoxidation of Allylehlorides with Hydrogen Peroxide over TS-1. In: Hattori H, Otsukak.Studies in Surface Science and Catalysis (Vol. 121). Tokyo: Kodansha Ltd, 1999. 355-358
  • 6清华大学.一种纳米级钛硅分子筛及其合成工艺.中国,CN1426962A.2003
  • 7Bartsch Richard A, Bitalac Leah P, Cowey Charles L, et al. Lariat ether alcohols based on dibenzo - 16 - crown - 5 [J]. Journal of Heterocyclic Chemistry, 2000,37 ( 5 ), 1337 - 1350.
  • 8Patel K M , Stevenson , Thomas M. 6 - alkoxy - 3 - ( 1,1 - dimethylethyl ) - 5,6 - dihydro - 4H - oxazine derivatives, a method for their preparation and their use as herbicides [ P ]. WO 9209587,1992 -06 - 11.
  • 9M Hamamoto, K Nakayama, Y Nishiyma, et al. Oxidation of organic substrates by a molecular oxygen/aldehyde/ heteropolyoxometalate system [ J ]. J. Org. Chem. , 1993, 58(23 ) :6421 -6425.
  • 10Carlo Venturello, Mario Gambaro. A convenient catalytic method for the dihydroxylation of alkenes by hydrogen peroxide [ J ]. Synthesis, 1989, (4) : 295 - 297.

引证文献3

二级引证文献4

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部