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2-氯-5-三氟甲基苯胺及其Schiff碱的合成与表征 被引量：1

Synthesis and Characterization of 2-Chloro-5-trifluoromethylaniline and Its Schiff Base
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摘要 以对氯三氟甲苯为原料,经硝化反应和金属还原,合成了2-氯-5-三氟甲基苯胺;再将2-氯-5-三氟甲基苯胺与不同的芳香醛反应,合成了2-氯-5-三氟甲基苯胺Schiff碱,产率达到68%-85%,对合成Schiff碱的结构进行了红外光谱、紫外光谱、核磁共振、质谱表征. 2-Chloro-5-trifluoromethylaniline were synthesized from p-ehlorobenzotrifluoride via nitration and reduction of metals. 2-Chloro-trifluoromethylaniline schiff base were synthesized through reaction of 2- chloro-5-trifluoromethyl aniline and aromatiealdehydes with yields of 68 % - 85 % ,Finally, Schiff base were characterized by IR, UV,IHNMR and MS determination.
作者 孟德素
机构地区 菏泽学院化学与化工系
出处 《信阳师范学院学报（自然科学版）》 CAS 北大核心 2013年第4期563-565,共3页 Journal of Xinyang Normal University(Natural Science Edition)
基金 山东省教育厅高校科研发展计划项目(J11LB58)
关键词 对氯三氟甲苯 3-硝基-4-氯三氟甲苯 2-氯-5-三氟甲基苯胺 SCHIFF碱 p-chlorobenzotfifluoride 3-nitro-4-chlorobenzotrifluoride 2-chloro -5-trifluoromethylani- line Sehiff base
分类号 O641.4 [理学—物理化学]
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引证文献1

信阳师范学院学报（自然科学版）
2013年 第4期

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