摘要
以对氯三氟甲苯为原料,经硝化反应和金属还原,合成了2-氯-5-三氟甲基苯胺;再将2-氯-5-三氟甲基苯胺与不同的芳香醛反应,合成了2-氯-5-三氟甲基苯胺Schiff碱,产率达到68%-85%,对合成Schiff碱的结构进行了红外光谱、紫外光谱、核磁共振、质谱表征.
2-Chloro-5-trifluoromethylaniline were synthesized from p-ehlorobenzotrifluoride via nitration and reduction of metals. 2-Chloro-trifluoromethylaniline schiff base were synthesized through reaction of 2- chloro-5-trifluoromethyl aniline and aromatiealdehydes with yields of 68 % - 85 % ,Finally, Schiff base were characterized by IR, UV,IHNMR and MS determination.
出处
《信阳师范学院学报(自然科学版)》
CAS
北大核心
2013年第4期563-565,共3页
Journal of Xinyang Normal University(Natural Science Edition)
基金
山东省教育厅高校科研发展计划项目(J11LB58)