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胶州湾海域海水中有机锡化合物含量的在线测定 被引量：1

Online determination of organotin in Jiaozhou gulf sea water
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摘要 对胶州湾海域海水中有机锡化合物进行了实时在线测定,利用船载海水有机锡自动测定仪,采用氢化物发生顶空固相微萃取-毛细管气相色谱-火焰光度检测器联用技术测定该海域海水中有机锡化合物的含量。测定结果表明,在胶州湾海域不同地点均检测出不同浓度的氯化三丁基锡,表明胶州湾海域中已经不同程度地受到了有机锡的污染。 Tributyltin in Jiaozhou gulf sea water is determined online by automatic analyzer,which is applied to measure the organotin in seawater with multiple coupling techniques like HSSPME-GC-FPD.The result indicates that different concentrations of tributyltin in selected sea areas are detected.It shows that the sea water in Jiaozhou gulf has been polluted by tributyltin.
作者 刘魁 张二琴 周长杰 赵家贺 李景印 史会英
机构地区 河北科技大学理学院 石药集团中诺药业(石家庄)有限公司
出处 《河北科技大学学报》 CAS 2013年第6期511-516,共6页 Journal of Hebei University of Science and Technology
基金 国家863项目(2007AA09210110)
关键词 氯化三丁基锡 自动测定仪 在线 海水 顶空固相微萃取-毛细管气相色谱-火焰光度法 tributyltin automatic analyzer online seawater HSSPME-GC-FPD
分类号 O657.63 [理学—分析化学]
  • 相关文献

参考文献15

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二级参考文献19

  • 1原现瑞,王玉春,田宝勇,胡丽丽,马桂娥.毛细管气相色谱法测定无公害柿子中菊酯类农药的残留量[J].河北科技大学学报,2005,26(4):272-274. 被引量：4
  • 2刘红梅,周庆霞,杨文玲.毛细管气相色谱法测定银杏叶中萜内酯含量[J].河北科技大学学报,2006,27(3):209-213. 被引量：6
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  • 10JIANG G B, CEULEMANS M, ADAMS F C. Optimization study for the speciation analysis of organotin and organogermanium compounds by on-column capillary gas chromatography with flame photometric detection using quartz surface-induced luminescence[J]. J Chromatogr, 1996,727 : 119-129.

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河北科技大学学报
2013年 第6期

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