摘要
在不同粗糙度和硬度的GCr15轴承钢基体上,利用多弧离子镀技术低温(175℃)沉积TiAlCN涂层.利用扫描电子显微镜(SEM)、AFM、EPMA、XRD和附着力测试仪等研究了薄膜形貌和性质.结果表明:基体越平整,制备的涂层表面也就越平整;薄膜附着力随着表面粗糙度的增大而减小,在基体粗糙度为0.01μm时,薄膜附着力达到最大值42.8N;基体硬度越高,膜/基附着力越大,在基体硬度为835HV0.01时,附着力达到最大值31.2N;在涂层中,发现了晶体结构为fcc-TiN结构,衍射图中没有AlN相出现,这是TiN相优于AlN相而形成的缘故.
The composite TiAlCN coatings were deposited by vacuum arc ion plating on GCr15 rings with different matrix materials hardness and roughness at 175 ℃ .The analysis results of SEM ,AFM ,EPMA ,XRD ,adhesion tester indicated :as the substrate surface roughness ,the preparation of the coating surface would be smooth .Film adhesion decreased with the increased of surface roughness .When the roughness was 0 .01 μm ,the film adhesion was up to the maximum of 42 .8 N .The higher the hardness of matrix ,the greater the adhe-sion of film/substrate was obtained .As the substrate hardness was 835 HV0 .01 ,the maxi-mum adhesion was 31 .2 N .The crystal structure of fcc-structure of TiN was found in the film .The diffraction pattern without AlN phase ,it was because of TiN phase was better than that of AlN phase formation .
出处
《陕西科技大学学报(自然科学版)》
2014年第1期74-77,共4页
Journal of Shaanxi University of Science & Technology
基金
陕西省教育厅产业化中试项目(2011TG24)
陕西科技大学研究生创新基金项目