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菲醌衍生物的合成及表征

Synthesis and Characterization of Phenanthrenequinone Derivatives
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摘要 从9,10-菲醌出发,通过溴化得到2,7-二溴-9,10-菲醌,通过两种不同的还原方式分别合成了不同的菲醌衍生物2,7-二溴-9,10-二羟基氢化菲和2,7-二溴9,10-二羟基菲.所得化合物通过1H NMR、13C NMR、ESI-MS和熔点测定等手段对其结构进行了表征. 2, 7-Dibromo-9, 10-phenanthrenequinone was synthesized from 9, 10-phenanthrenequinne by bromination, and then prepared two different phenanthrenequinone derivatives: 2, 7-dibromo-9, 10-dihydroxy dihydrophenanthren and 2, 7-dibromo-9, 10-dihydroxy phenanthrene by two differrent ways of reduction. Their structures were characterized by H NMR, 13C NMR, ESI-MS and melting points.
出处 《河南科学》 2013年第12期2137-2139,共3页 Henan Science
基金 河南省基础与前沿技术研究计划项目(122300410090)
关键词 菲醌 2 7-二溴菲醌 菲醌衍生物 合成 phenanthrenequinone 2,7-Dibromo-phenanthrenequinone: phenanthrenequinone derivatives synthesis
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