4-氨基-3-肼基-5-巯基-1,2,4-三唑的微波合成方法

Microwave Synthetic Method of 4-Amino-3-Hydradzino-5-Mercapto-1, 2, 4-Triazole

本文采用微波合成技术,以水合肼和硫脲为原料一步合成得到4-氨基-3-肼基-5-巯基-1,2,4-三唑(AHMT),并对最佳合成条件进行了摸索。考查了反应时间,微波功率,反应物用量对产率的影响。

by using hydrazine hydrate and thiourea as the raw material, 4- amino -3- hydrazine -5- mercapto -1, 2, 4- triazole was synthesized in one step by microwave. The optimum conditions were studied, including the effects of reaction time, microwave power, influence of reactant amount on the yield.