摘要
本文以气相色谱法测定乙草胺与 2,4-D丁酯混合制剂中各组分含量。采用 Φ3mm x2m的不锈钢柱,内填充物为5%OV-101/101白色硅烷化担体,邻苯二甲酸二正丁酯为内标物。变异系数小于1%,乙草胺平均回收率为99.3%,2,4-D丁酯平均回收率99.0%。方法用于实际测定,结果令人满意。
The paper introduces the method of determinating contents of acetofonate and 2. 4 - dichlorophenoxyacetate with chromatography adopting stainless steel column of φ3mm x 2m with packing material of 5% OV- 101/101 white silanization in it,dibutyl phthalate is internal stundard reagent, the changing coeflicient is less than 1 %. The recovery of acetofenate and 2,4 - dichlorophenoxyacetate is individualy 99.3% and 99.0%. Determinating in this method, the result is satisfied.
出处
《化学工程师》
CAS
2000年第6期50-51,共2页
Chemical Engineer
关键词
气相色谱
测定
乙草胺
丁酯
除草剂
含量
Chromaography
Determination
Acetofenate
2,4 -Dichlorophenoxyacetate.