摘要
采用薄层色谱法分离己基葡萄糖苷(APG-06),并对分离的各组分进行核磁共振氢谱(1HNMR)鉴定。结果表明,以氯仿/无水乙醇/氨水(V(氯仿)∶V(无水乙醇)∶V(氨水)=19∶13∶1)混合溶液为展开剂可将APG-06在薄层板上分成5个区段;5个区段的组分分别为原料醇、单苷、二苷、三苷、四苷及以上与多聚糖的混合物。
The various components in hexyl glucoside (APG -06) product sample were separated by thin layer chromatography (TLC), and identified by 1HNMR. Results Showed that when mobile phase consists of V(CHCl3) : V(CH3CH2OH) : V( NH3. H2O) = 19:13 : 1, the APG - 06 product can be separated into five parts: unreacted alcohol, monoglucoside, diglucoside, triglucoside and polyglucosides that are higher than tetraglucoside.
出处
《日用化学工业》
CAS
CSCD
北大核心
2014年第3期171-173,179,共4页
China Surfactant Detergent & Cosmetics
基金
山西省青年科技研究基金资助项目(No.2011021010-2)
山西省科技创新基金资助项目(No.2012102008)