摘要
目的:建立活血止痛片的质量控制方法。方法:采用薄层色谱法对活血止痛片中的赤芍、当归、三七进行鉴别;采用高效液相色谱法对活血止痛片中的芍药苷进行定量。结果:赤芍、当归、三七薄层色谱斑点清晰,阴性无干扰;芍药苷在51.52~1288.0ng的范围内呈良好的线性关系,r=0.99995,平均加样回收率为99.79%,RSD=1.21%。结论:该方法简便准确,重现性好,可作为活血止痛片的质量控制标准。
Objective: To establish the quality standards of Huoxuezhitong tablet. Methods: TLC was used to distinguish the Radix Paeoniae Rubra, Radix Angelicae sinensis and Radix Notoginseng in Huoxuezhitong tablet; The content of paeoniflorin was determined by HPLC. Results: The prescription of Radix Paeoniae Rubra, Radix Angelicae sinensis and Radix Notoginseng has distinguishing characteristics without the interference of the blank control. Paeoniflorin in the framework of 51.52-1288.0ng showed a good linear relationship, r=0.9999, the average recovery was 99.79%, RSD=1.21%. Conclusion: This method is simple, accurate and reproducible, it can be used to control the quality of Huoxuezhitong tablet.
出处
《按摩与康复医学》
2014年第3期144-147,共4页
Chinese Manipulation and Rehabilitation Medicine