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Azide-functionalization of carbon nanotubes by electrochemical oxidation of N_3^-in situ 被引量:1

Azide-functionalization of carbon nanotubes by electrochemical oxidation of N_3^- in situ
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摘要 Azide-functionalization of single-walled carbon nanotubes (SWCNTs) was achieved by electrochemical oxidation of N3 in situ. The functionalized nanotubes were characterized in details by single internal reflection infrared spectroscopy (ATR-FTIR) and thermogravimetic analysis (TGA/MS). The results revealed that a covalent C-N bond had formed and this might provide an effective method for the preparation of azide-functionalized materials, especially carbon materials. The degree of functionaliza- tion was measured by X-ray photoelectron spectroscopy (XPS). Azide-functionalization of single-walled carbon nanotubes (SWCNTs) was achieved by electrochemical oxidation of N3 in situ. The functionalized nanotubes were characterized in details by single internal reflection infrared spectroscopy (ATR-FTIR) and thermogravimetic analysis (TGA/MS). The results revealed that a covalent C-N bond had formed and this might provide an effective method for the preparation of azide-functionalized materials, especially carbon materials. The degree of functionaliza- tion was measured by X-ray photoelectron spectroscopy (XPS).
出处 《Chinese Chemical Letters》 SCIE CAS CSCD 2014年第2期292-294,共3页 中国化学快报(英文版)
关键词 Electrochemical treatment Carbon nanotubes AZIDE Eunctionalization Electrochemical treatment Carbon nanotubes Azide Eunctionalization
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