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汽油样品预处理方法的探讨─汽油中痕量铅的测定 被引量:3

The Study of the Pretreatment Method for the Gasoline Samples The Determination of Lead in Gasoline
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摘要 研究了测定汽油中痕量铅时两种预处理- 测定方法: (1) 碘- 正辛醇萃取- 硝酸反萃取- 离子交换、洗脱后用阳极溶出法测定; (2) 微波提取- 原子吸收法测定。对两种方法的最佳条件进行了讨论。 Two kinds of pretreatment method were studied for the determination of trace lead in gasoline:(1)The lead in gasoline was extracted by iodine-1-octanol,reverse-extracted by nitric acid,exchanged by ion exchanger,eluted by hydrochloric acid and determined by Anodic Stripping Voltammetry (ASV).(2)The lead in gasoline was extracted by nitric acid in a WR-1 microwave sample treatment system and then determined by atomic absorption spectrometery(AAS).Some conditions for both method (1) and (2) were optimized.
出处 《江苏石油化工学院学报》 1999年第4期4-7,共4页 Journal of Jiangsu Institute of Petrochemical Technology
基金 江苏省自然科学基金
关键词 汽油铅 预处理 阳极溶出法 原子吸收 测定 痕量 Lead gasoline Pretreatment ASV AAS
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