摘要
以甲醛、异丁醛为主要原料,开展了2 ,2 - 二甲基- 1 ,3 - 丙二醇羟基特戊酸单酯的小试合成研究,考察了物料配比、温度、反应时间、催化剂用量等因素对反应的影响,产品总收率大于75 % ,纯度99 % 以上。
Dimethyl-3-hydroxypropyl 2,2-dimethyl-3-hydroxypropanoate was synthesized with formaldehyde and isobutylaldehyde as raw materials. The effects of reactants ratio, temperature, time and catalysts on the reaction were studied. The yield of the product was over 75%. The purity of the product was 99% and over.
出处
《石化技术与应用》
CAS
1999年第3期142-144,共3页
Petrochemical Technology & Application
关键词
甲醛
二甲基
丙二醇羟基特戊酸单酯
缩合
formaldehyde
isobutylaldehyde
2,2-dimethyl-3-hydroxypropyl 2,2-dimethyl-3-hydroxypropanoate
condensation