摘要
目的:分析不同贮藏年份新会陈皮中挥发性成分的组成和含量,考察贮藏时间对新会陈皮中挥发性成分的影响。方法:采用GC-MS法测定了1983-2012年22批不同贮藏年份的新会陈皮样品,运用函数拟合方法对所得数据与年份的相关性进行了统计分析。结果:除2-甲氨基-苯甲酸甲酯外,其他主要挥发油成分的含量未随贮藏年份增加而呈现下降趋势。β-月桂烯与2-甲氨基-苯甲酸甲酯峰的含量比值与贮藏年份的对数函数相关性达到0.86以上。结论:陈皮"陈久者良"的说法难以用其中挥发性成分含量变化来佐证,但是新会陈皮中β-月桂烯峰与2-甲氨基-苯甲酸甲酯含量比值对陈皮年份鉴别有参考意义,有助于完善广陈皮的质量控制。
Objective:To analyze the composition and content of volatile components of Xinhui Pericarpium Citri Reticulate (PCR) of different storage time.Investigate the influence of storage time on the volatile components.Method:Twenty-two samples of different storage time (from 1983 to 2012) were analyzed by GC-MS.The correlation of the data and the storage time was studied through statistical analysis by function fiftting method.Result:The contents of the major components did not decrease dramatically with the storage time except 2-methylamino-benzoic acid methyl ester.It was found that the content ratio ofβ-myrcene to 2-methylaminobenzoic acid methyl ester changed logarithmically with the storage time.The correlation could reach more than 0.86.Conclusion:It was able to confirm that ‘ longer storage time the better’ for the PCR with the change of the contents of volatile components.However the content ratio ofβ-myrcene to 2-methylamino-benzoic acid methyl ester supply evidence for the identification of storage time of Xinhui PCR,and will improve the quality control of Xinhui PCR.
出处
《中国实验方剂学杂志》
CAS
北大核心
2014年第9期62-65,共4页
Chinese Journal of Experimental Traditional Medical Formulae
基金
国家自然科学基金青年基金项目(81102782)
2011年中国博士后科学基金项目(2011M501368)