摘要
以富马酸和十二醇为原料,对甲苯磺酸为催化剂,合成了富马酸双十二酯。运用正交实验法考察了反应时间、反应温度、原料配比及催化剂用量对酯化的影响。
The di - dode Canol fumaroid was prepared by ester reation using P - toluene sulphonic acid as catalyst,Fumaric acid and dodecyl alcohol are raw materials for the ester realtion, the effeet faters for the ester reaction, Suchas: reaction tiom, temperature, raw material ration and amount of the catalyst were investigated through orthogonal test.
关键词
富马酸双十三酯
富马酸
十二醇
对甲苯磺酸
正交实验
di - do decanol fumaroid
fumaric acid
dodecyl alcohol
P - toluene sulphonic acid
orthogonal test.