摘要
采用高效液相色谱法测定补肾强身胶囊中淫羊藿苷的含量。以XB-C18为色谱柱,以乙腈-水(30∶70)为流动相,以270nm为检测波长,流速为1.0ml/min,柱温为30℃。淫羊藿苷在16.576-165.76ug/ml的浓度范围内线性关系良好,R^2=1,平均回收率为100.2%,RSD%为0.74%。该方法简便、快捷、准确,能有效地控制补肾强身胶囊的质量。
Using high performance liquid chromatography (HPLC)method was developed for the determination of epimedium glycoside in kidney and strengthen the capsule content. For XB - C18 chromatographic column, with acetonitrile - water (30∶70)as mobile phase, detection wavelength for 270nm, the flow rate of 1.0 ml/min, column temperature 30℃. Epimedium glycoside in 16.576 to 165.76ug/ml concentration range inside sex good, R^2=1, the average recovery was 100.2%, RSD % to 0.74%. The method is simple, quick, accurate, and can effectively control the quality of the kidney and strengthening the capsule.
出处
《北方药学》
2014年第6期1-2,共2页
Journal of North Pharmacy
关键词
高效液相色谱法
补肾强身胶囊
淫羊藿苷
High performance liquid chromatography
Kidney and strengthen the capsule
Epimedium glycoside