摘要
目的:研究龙须草的化学成分。方法:采用各种柱色谱法分离其成分,运用多种波谱方法鉴定化合物结构。结果:从龙须草的乙酸乙酯部位共分离得到8个化合物,分别鉴定为:2-羟基-3-甲基蒽醌(1)、大黄素甲醚(2)、豆甾醇(3)、豆甾-3,6-二酮(4)、香草醛(5)、正二十七烷酸(6)、反式对羟基桂皮酸(7)、4-羟基-3-甲氧基苯甲酸(8)。结论:其中,化合物1、2、4、6为首次从该属植物中分离得到,化合物1~8均为首次从该植物中分离得到。
Objective: To study the chemical constituents of Juncus setchuensis.Methods: Column chromatography was used in the isolation procedure.The structures of isolated compounds were elucidated by spectral data.Results: Eight compounds were isolated and their structures were identified as 2-hydroxy-3-methylanthraquinone( 1),physcion( 2),stigmasterol( 3),stigmast-3,6-dione( 4),vanillin( 5),n-heptacosanoic acid( 6),trans-hydroxycinnamic( 7) and 4-hydroxy-3-methoxy benzoic acid( 8).Conclusion: Compound 1,2,4 and6 are obtained from this genus for the first time and all the compounds are obtained from this plant for the first time.
出处
《中药材》
CAS
CSCD
北大核心
2014年第4期602-604,共3页
Journal of Chinese Medicinal Materials
基金
南京军区科技创新课题(11MA058)
关键词
龙须草
化学成分
Juncus setchuensis Buchen. Chemical constituents