摘要
C_(14)H_(20)N_3O_2PS_2, M_r = 357. 44, monoclinic, space group P21/c, a =10. 825(2) . b=10. 511(2) , c=16. 402(1) ,β=102. 12(1)°,V=1824. 8 ￣3 . Z=4, D_x= 1. 30 g/cm￣3 , μ=3. 74 cm￣(-1), and F(000) = 376. R(R_w) is 0. 051 (0. 063) for1599 observed unique reflections.The five-membered thiazolinone is planar group. andthe dihedral angle between it and the six-membered phenyl is 64. 2°.
C_(14)H_(20)N_3O_2PS_2, M_r = 357. 44, monoclinic, space group P21/c, a =10. 825(2) . b=10. 511(2) , c=16. 402(1) ,β=102. 12(1)°,V=1824. 8 ￣3 . Z=4, D_x= 1. 30 g/cm￣3 , μ=3. 74 cm￣(-1), and F(000) = 376. R(R_w) is 0. 051 (0. 063) for1599 observed unique reflections.The five-membered thiazolinone is planar group. andthe dihedral angle between it and the six-membered phenyl is 64. 2°.
