(C_(12)H_8N_2)_2MnCl_2晶体的水热合成与表征

Hydrothermal Synthesis and Characterization of (C_(12)H_8N_2)_2MnCl_2

用水热方法合成 (C12 H8N2 ) 2 Mn Cl2 晶体 ,并用 X射线衍射仪对其结构进行表征 .该晶体属单斜晶系 ,P2 1/c空间群 ,a=0 .9472 (2 ) nm,b=1 .52 0 36(1 1 ) nm,c=1 .452 7(2 ) nm,α=γ=90°,β=98.96(2 )°,V=2 .0 664(6) nm3,Z=7.

A crystal of (C 12 H 8N 2) 2MnCl 2 was synthesized by the hydrothermal method and characterizated by single-crtstal X-ray structure diffraction. The title compound crystallized in a monoclinic system, its space group was P2 1/c with a=0 947 2(2) nm, b=1 520 36(11) nm, c=1 452 7(2) nm, \{α=γ=90°\}, β=98 96(2)°, V=2 066 4(6) nm 3, Z=7.