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人尿中克罗帕米的GC/MSD检测方法研究

Determination of Clopamide in Human Urine by GC/MSD
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摘要 建立了人尿中克罗帕米的GC/MSD的检测方法 ,发现了三种甲基化产物。比较了不同的提取方法 ,碱性提取收率可达 94 5 %。 Clopamide as a new diuretic was forbidden by IOC.A new reliable GC/MSD determination method of clopamide in human urine is described in this paper.Three methyled compounds are found and varieties of extraction procedures are compared.The basic extraction recovery is 94.5%. The excretion profile of clopamide in human urine has been investigated.Clopamide could be detected in human urine within 20 hours.
出处 《质谱学报》 EI CAS CSCD 2001年第1期21-24,共4页 Journal of Chinese Mass Spectrometry Society
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  • 1[1]The banned list of abused drugs in sports 1997,Jan
  • 2[2]Fullinfaw RO,Bury RW,Moulds RF.Liquid chromatographic screening of diuretics in urine. J Chromatogr. 1987, Apr 10,415(2) :347 - 56
  • 3[3]Sane RT,Sadana GS,Bhounsule GJ et al. High- performance liquid chromatographic determination of xipamide and clopamide in phannaceuticals.J Chromatogr. 1986,Apr 18,356(3):468-72

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