摘要
建立了 2 0 %增效可溶性噻枯唑 ( MBAMT)粉剂中有效成分 MBAMT的高效液相色谱 ( HPLC)分析方法。采用硅胶柱 ,正已烷∶无水乙醇 =9∶ 2 ( V/V )为流动相 ,所得结果良好 ,平均回收率为 93.75 % ,变异系数为 2 .1 8%。方法简易、快速、准确 。
The HPLC method for determination of MBAMT(N,N′ methylene bis(2 amino 5 mercapto 1,3,4 thiadia zole)has been reported. The sample was analyzed on a SiO 2 column with mobile phase of n hexane∶ethyl alcohol=9∶2( V/V )using UV detector at 320 nm. The variation coefficient, recovery were 2.183% and 93.76%, respectively. The analytical results show that this method is simple, rapid and accurate.
出处
《分析科学学报》
CAS
CSCD
北大核心
2001年第2期131-134,共4页
Journal of Analytical Science
