摘要
目的:研究麻甘合剂的质量标准,方法:流动相为乙腈-三乙胺-磷酸-水谱法(TLC)和盐酸麻黄碱的高效液相(1.8∶0.1∶0.1∶9.8),检测波长为214 nm,样品提取过滤后进行分析。色谱法(HPLC)。建立杏仁、甘草的薄结果:线性范围20~200 μg·ml-1,相关系数r=0.9996,精层色密度为1.20%,加样回收率100.34%。结论:该方法适用于麻甘合剂的质量控制。
OBJECTIVE:The quality standards for OBbeen studied.The TLC methods for prunus armeniaca and Glycyrrhiza uralensiJECTIVE:The quality standards for mistura ms were establishedliquid chromatographic method was established for determination of Ephedri.A simple high performance agan have mistura magan ne Hydrochloride.METHOD was acetonitrile-triethyphoat 214nm.The sample was extracted by mobile phase.ric acid-water(1.8∶0.1∶0.1∶9.8).The UV dectector was set lammine-RESULTS:The linear range was f=0.9996.The relative standard deviation was 1.20%.The rom 20~200 μg·ml-1, r phosS:The mobile phase recovery was 100.34%.CONCLUSIONS:The method is suitable for the quality standards of mistura magan .
出处
《中国医院药学杂志》
CAS
CSCD
北大核心
2001年第3期155-157,共3页
Chinese Journal of Hospital Pharmacy