摘要
本文采用Seppak C_(18)小柱固相萃取鸦片中的五种主要成分,以反相高效液相色谱法,甲醇—甲酸—三乙胺水(35:1.5:0.5:63)为流动相,检验五种成分,各成分均有良好的回收率。方法简单、快速、准确。
A simple and rapid method for the isolation and detection of five major alkaloids in opium by Sep --pak C_(18) cartridges sol(d--phase extraction and high--performance liquid chromatography is reported. The recoveries by using of the eartridage were excellent for most alkaloids. Separation of each alkaloid peak from each other on the high--performance liquid chromatography was satisfactory by using of μ--Bondapak C_(18) column and methanol--methanoic acid--triethylamine--water (35: 1.5: 0.5: 63,v/v) as mobile phase.
出处
《中国法医学杂志》
CSCD
1993年第3期154-155,共2页
Chinese Journal of Forensic Medicine
