脲系磷化合物的研究(Ⅸ)——脲基硫代磷酰胺酯和双脲基硫代磷酸酯的合成

STUDIES ON PHOSPHORUS SUBSTITULED UREA COMPOUNDS Ⅸ. Synthesis of Ureidophosphoramidothioates and Bis-(Ureido)phosphorothioates

合成了八种新的脲基和双脲基硫代磷酸酯,其化学式为[RO(H_2N)P(S)NHCONHCOC_(?)H_(?)]和[ROP(S)(NHCONHCOC_(?)H_(?))_2]。利用红外光谱和核磁共振谱对目标化合物进行了表征,并对目标化合物的~1H NMR特性进行了讨论。

Eight new compoumds ureidophosphoramidothioates and his-(uicrdo)phosphorothioatos wore synthesizod, with genoral formula [RO(H_2N)P(S)NHCONHCOC_6H_5]and[ROP(S) (NHCONHCOC_6H_5)_2]. The title compounds have been characterized by IR and ~1HNMR. Their characteristic properties of NMR aro also discussed.