摘要
研究了用三氯化磷和正丁醇合成亚磷酸二正丁酯的方法 ,讨论了原料配比、反应时间、温度、溶剂用量等因素对反应的影响 ,确定了合成亚磷酸二正丁酯的最佳反应条件 ,在选择的试验条件下产率为 97 1%。
A method for preparing dibutyl phosphite was developed from n[KG-4]-butanol and phosphorus trichloride.The effects of reactant ratio,time,temperature and solvents on the reactions were examined.The optimal reaction conditions were determined.The yield of the product can be up to 97 1%。 [
出处
《石油化工》
CAS
CSCD
北大核心
2001年第4期293-295,共3页
Petrochemical Technology
