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分析裂解衍生化技术及其在刑事技术中的应用 被引量:5

ANALYTICAL PYROLYSIS DERIVATIZATI ON TECHNIQUE AND ITS APPLICATIONS IN FORENSIC SCI ENCE
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摘要 介绍了近年来分析裂解衍生化反应技术,如加氢还原法;基质修饰剂法;同时裂解甲基化法;同时热液分解法。并就该技术的现状、原理、进展及其在刑事技术中的应用进行了综述。 In this paper,analytical pyrolysis derivatization techniqus,included:(1)hydrogenation reduction;(2)matrix decoration;(3)simultaneous pyrolysis methylatio n and(4)simultaneous hydrothermal decomposition were intro-duced and the present,principle,pr ogression of the techniques and its a pplications in forensic science were reviewed.
出处 《刑事技术》 2001年第3期33-35,共3页 Forensic Science and Technology
关键词 分析裂解衍生化 刑事技术 高分子样品 气相色谱 分析技术 analytical pyrolysis,derivatization
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参考文献8

  • 1[1]J M Challinor. A pyrolysis- derivatisation- gas chromatography technique for the structural elucidation of some synthetic polymers. J of Anal Appl Pyrolysis, 1989, 16:323 ~ 333
  • 2[2]J. M. Challinor. The scope of pyrolysis methylation reactions. J ofAnal Appl Pyrolysis, 1991, 20:15 ~ 24
  • 3[3]S Tsuge, etal. Structural characterization of polyolefins by pyrolysis- hydrogenation glass capillary gas chromatography. J of AnalAppl Pyrolysis, 1980, 1:221 ~ 229
  • 4[4]M Hida, etal. Curie - point pyrolysis - gas chromatography of aliphaticamines in the presence of metal powder and inorganic salt. J of AnalAppl Pyrolysis, 1990, 17:181 ~ 188
  • 5[5]A. Onishi, etal. Simultaneous hydrothermal decomposition andderivatizations: gas chromatography/mass spectrometry for the characterization of polyamindes. Anal Sci, 1994, 10:271 ~ 276
  • 6[6]肥田宗政, etal. Pyrolysis -GC and GC/MS for determination ofglyphose in human blood. Bunseki Kagaku, 1989, 38:87 ~ 91
  • 7丁军凯,闫福宁,喻晓光,宋鸣,邹天治,范垂昌,孙中芙.同时裂解甲基化气相色谱法快速鉴别人体脂肪及动植物油脂[J].中国法医学杂志,1998,13(4):227-230. 被引量:14
  • 8[8]Ding junkai, etal. The effect of insomerization and degradation ofpolyunsaturatde fatty acids from oils by different volume proportionsof tetramethylammonium hydroxide in thermally assisted hydrolysisand methlation. J of Anal Appl Pyrolysis, 1997, 42: 1 ~ 8

二级参考文献2

共引文献13

同被引文献33

  • 1丁军凯,黄丽,宋鸣,孙玉梅.裂解氢化技术在鉴别聚烯烃类塑料中加氢催化剂用量的最佳化研究[J].现代仪器,2004,10(6):18-19. 被引量:1
  • 2赵海珍,陆兆新,别小妹,吕凤霞.高效液相色谱法测定猪油甘油三酯中的脂肪酸位置分布[J].色谱,2005,23(2):142-145. 被引量:38
  • 3张旭,董晓萍,邓斌贝,郭平,陈海红,江道峰,王曙.GC-MS分析蜣螂油脂的化学成分[J].华西药学杂志,2006,21(3):247-248. 被引量:17
  • 4李浩春.气相色谱法[M].北京:科学出版社,1998.248.
  • 5[1]Challinor J M. The scope of pyrolysis methylation reactions[J]. J Anal Appl Pyrolysis, 1991, 20:15~24.
  • 6[8]Ding Junkai, et al. The effect of isomerization and degradation of polyunsaturated, fatty acids from oils by different volume proportions of tetramethylammoneous hydroxide in thermally assisted hydrolysis and methylation[J]. J Anal Appl Pyrolysis, 1997,42:1~8.
  • 7[1]Schooten JV,Evenhuis JK.Pyrolysis-hydrogenationGLC of alpha olefin copolymers[J].Polymer,1965,6:561-577.
  • 8[2]Michajlov L,Zugenmaier P,Cantow H J.Structural investigation on polyethylenes and ethylene-propylene copolymers by reaction gas chromatography and X-ray diffraction[J].Polymer,1968,9:325-343.
  • 9[3]Sugimura Y,Nagaya T,Tsuge S.Microstructural characterization of polypropylenes by high-resolution pyrolysis-hydrogenation glass capillary gas chromatography[J].Macromolecules,1980,13:928-932.
  • 10[4]Tsuge S,Sugimura Y,Nagaya T.Structural characterization of polyolefins by pyrolysis-hydrogenation glass capillary gas chromatography[J].J.Aanl.and Appl.Pyrolysis,1980,1:221-229.

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