四硝基二苯并-1,3a,4,6a-四氮杂戊搭烯合成工艺改进

The Improvement of Synthetical Technics of Tetranitrodibenzo-1,3a,4,6a-Tetrazapentalene

采用经改进的四硝基二苯并 - 1,3a,4,6 a-四氮杂戊搭烯 (代号为 TACOT)的合成工艺 ,将 TACOT的合成总时间缩短了一半 ,简化了合成操作 ,将产物的总得率由 2 6 .7%提高至 5 2 .0 % ,从而大大降低了

TACOT was synthesized by the improved technics, the time of reaction was shortened to a half, and the operation was predigested. Moreover, the total yields have been increased from 26.7% to 52.0%. This methods reduced the cost of TACOT greatly.