N-(-3’-氨基4’-溴代)苯甲酰-2-甲基-5-溴代苯胺的合成

Synthesis of N-(3'-amino-4'-bromo) benzoyl-2-methyl-5-bromo aniline

以 4 溴甲苯为初始原料 ,经过氧化 ,硝化 ,缩合 ,还原反应 ,制成有机颜料中间体N ( 3’ 氨基 4’ 溴代 )苯甲酰 2 甲基 5 溴代苯胺。对影响反应的各种因素进行了讨论 ,产品总收率为 5 7 8% .

Through using 4 bromomethylbenzene as the first meaterial,an organic pigment intermediate N (3' amino 4' bromo)benzoyl 2 methyl 5 bromo aniline was synthesized by oxidation,nitration,condenstaion,reduction.Some parameters were discussed.The total yield is 57.8%.