摘要
本文研究了流动注射氢化物发生-蒸气贮存脉冲进样原子荧光法测定地质样品中痕量砷的方法。砷的灵敏度提高17.6倍,精密度(RSD)为2.1%,检出限为0.32ng/mL。用于地质标准样的测定,结果满意。
A method for the determination of trace arsenic in geological samples by flow injection hydride generation vapor store and pulsed sampling atomic fluorescence spectrometry has been developed. The performances of two kinds of vapor store system have been compared with.The analytical sensitivity of arsenic has incrested by 1760 percent,The detection limit is 0.32ng/mL and relative standard deviation (RSD)2.1%.Analytical results of geological stsndard reference materials are satisfactory.
出处
《光谱实验室》
CAS
CSCD
1998年第5期28-31,共4页
Chinese Journal of Spectroscopy Laboratory