摘要
确立了以 AC 20石英毛细管柱为分离柱的气相色谱分析方法采用面积归一法定量。该法简便,分析时间短,准确度高,完全可以满足SH/T 1489—92《对二甲苯》中各组分分析的精度要求。
出处
《化工标准.计量.质量》
2001年第6期21-22,共2页
Chemical Industry Standard·Measurement·Quality
同被引文献15
-
1Klemn E, Wang Jianguo, Emig G.A comparative study of the sorption of benzene and phenol in silicalite, HAlZSM-5 and NaAlZSM-5 by computer simulation [ J ]. Microporous and Mesoporous Materials, 1998,26 ( 1 - 3) : 11 - 21.
-
2Song L, Sun Z L, Rees L V C. Experimental and molecular simulation studies of adsorption and diffusion of cyclic hydrocarbons in silicalite-1 [J]. Microporous and mesoporous material, 2002, 55 (1) : 31 - 49.
-
3Guo Guo-Qing, et al. Separation of p-xylene from C8 aromatics on binder-free hydrophobic adsorbent of MFI zeolite [J]. Microporous and mesoporous material, 2000, 39 : 149- 161.
-
4Song Lijuan. Advanced studies of diffusion and adsorption in zeolites using the frequency-response method [ D]. Edinburgh: University of Edinburgh, 1999, 57- 62.
-
5Douglas M, Ruthven, Bal K K. Adsorption of n-hexane and intermediate molecular weight aromatic hydrocarbons on LaY zeolite[J]. Ind Eng Chem Res, 1996, 35:2060- 2064.
-
6Veronique Cottier, Jean-Pierre Bellat, Marie-Helene S G.Adsorption of p-xylene/m-xylene gas mixtures on BaY and NaY Zeolites. Coadsorption equilibria and selectivities[J].J Phy Che B, 1997, 101:4798-4802.
-
7Mentzen B F, Gelin P. The silicatite/p-xylene systerm:part1-flexibility of the MFI framework and aorption mechanisrn observed during p-xylene pore-filling BY X-ray powder diffraction at room temperature [ J ]. Materials Research Bulletin, 1995, 30(3) :373 - 380.
-
8Robin E R, Lovat V C R. The motion of p-xylene in ZSM-5[J]. Zeolites, 1988, 8:35-39.
-
9Chung-Kung L, Anthoay S T C. Adsorption of aromatic compounds in large MFI zeolite crystals[J]. J Chem Soe,Faraday Trans. 1996, 92(18): 3445-3451.
-
10Shah P B, Guo C J, Hayhurst D T. Intracrystalline diffusion of benzene in silicalite: the effect of structural heterogeneity[J]. J Chem Soc Faraday Tram, 1995, 91(7):1143 - 1146.
-
1陆宽.气相色谱面积归一法测定氯乙酸甲酯[J].杭州化工,2002,32(2):36-38. 被引量:4
-
2黄英,金丽青.2,2′-双[4-(3-氨基苯氧基)苯基]丙烷的合成[J].化学世界,2008,49(4):229-232. 被引量:3
-
3宋春燕,许银根.1,1,1,3,5,5,5-七甲基三硅氧烷的定量分析[J].有机硅材料,2016,30(4):323-325. 被引量:1
-
4周志岐.气相色谱法分析MDEA-环丁砜-水脱硫溶液的组成[J].石油与天然气化工,1991,20(2):1-6. 被引量:3
-
5陈其清,蒲祖伦.对硝基氯苯的气相色谱分析[J].化工标准化与质量监督,2000(10):21-22.
-
6李倩怡,施淡淡,陈国敏.气相色谱法测定萘产品中的萘含量[J].燃料与化工,2015,46(3):37-39. 被引量:2
-
7朱轶军,苗夫传,崔群,王海燕.C_5贮运工艺条件研究[J].化学工程,2008,36(9):71-74.
-
8周波,赵军龙,刘涛,岳金彩.气相色谱-质谱联用测定DEIP中的微量组分[J].聚氨酯工业,2009,24(1):43-45. 被引量:1
-
9陈长生,刘贞玲.毛细管气相色谱测定芳烃组成[J].化学工业与工程技术,2008,29(1):59-60. 被引量:2
-
10翟淑红,黄少烈,顾志伟.茶树油的分子蒸馏精制及其GC/MS分析[J].广东化工,2008,35(1):97-100. 被引量:14