N-苄氧基邻苯二甲酰亚胺的合成

Synthesis of N-benzyloxyphthalimide

以N 羟基邻苯二甲酰亚胺、氯化苄和乙酸钠或三乙胺为原料 ,通过控制反应温度和反应时间高产率地制备了N

N benzyloxyphtalimide was synthesized by condensation of N hydroxyphthalimide and benzyl chloride, using sodium acetate or triethyl amine as HCl absorbent. The yield could reach about 85% in 3h at 120℃ when triethyl amine was used as HCl absorbent.