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巯基乙酸2-乙基己酯的合成 被引量:1

Synthesis of 2-Ethyl Hexyl Mercaptoacetate
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摘要 本文介绍了巯基乙酸2-乙基己酯产品的用途、性能以及合成路线。以2-乙基己醇和氯乙酸为起始反应原料,采用先酯化后巯基化的合成工艺,催化剂活性高、反应步骤少、产品收率高,解决了先巯基化后酯化工艺过程复杂、对巯基乙酸纯度要求高、生产成本高的难题,是具有较高工业化实践价值的新生产工艺。 The application, performance and synthesis route of 2-ethyl hexyl mercaptoacetate product are introduced in this article. The synthesis process which adopts esterification firstly, then sulfhydrylation is based on starting materials 2-ethyl hexanol and chloroacetic acid. The activity of the catalyst is high, reaction steps are few and overall yield of product is high. Difficulties including complex process of sulfhydrylation first and then esterification, requirement of high purity of mercaptoacetic acid, and high production cost have been overcome. This new manufacturing process has a high commercial value.
出处 《精细与专用化学品》 CAS 2001年第1期18-19,共2页 Fine and Specialty Chemicals
关键词 氯乙酸 2-乙基己醇 巯基乙酸2-乙基己酯 合成 chloroacetic acid, 2-ethyl hexanol, 2-ethyl hexyl mercaptoacetate
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