含Mo—O的无机/有机杂化晶体的水热合成与表征

HYDROTHERMAL SYNTHESIS AND CHARACTERIZATION OF INORGANIC/ORGANIC HYBRIDE CRYSTAL CONTAINING Mo-O CLUSTOR

用水热方法合成了Mo—O/EN的无机 /有机杂化晶体 ,并用X—射线衍射对其结构进行了表征 .该晶体属于单斜晶系 ,P2 (1 ) /n空间群 ,a =8.0 86(2 ) A ,b =1 4 .4 67(1 ) A ,c =8.92 0 (1 ) A ,β =98.1 5 2 (1 4 )°,V=1 0 3 2 .9(2 ) A3。

A hybride crystal containing Mo-O/EN has been synthesized by hydrothermal method and characterizated by single crystal X-ray structural diffraction.The crystal data for the title compound,monodinic,space group P 2(1)/n with a=8.086(2),b=14.467(1),c=8.920(1),β=98.152(14)°,V=1032.9(2) 3,z=8.