5-取代1,10-菲咯琳化合物的合成和表征(英文)

Synthesis and characterization of 5-substituted derivatives of 1,10-phenanthroline

合成了二种新的5-取代1,10-菲咯啉化合物phen-NHCO（CH2）nBr（n=9,11）,它们是高效的分析化学试剂、钌（Ⅱ）类电化学发光（ECL）传感器活性材料的配体。利用元素分析、红外光谱、核磁共振氢谱和激光解析电离飞行时间质谱确证了其组成和结构。

Two new 5-substituted 1,10-phenanthroline derivatives, phen-NHCO-(CH2)nBr(n =9,11)were prepared. Their chemical structures were confirmed by means of elemental analysis, infared spectra, proton nuclear magnetic resonance spectra and mass spectra.