摘要
目的 :研究银杏酸α1单体的制备技术。方法 :以乙醇为提取溶剂 ,获得的乙醇浸膏经硅胶吸附能除去大部分极性较大的杂质 ,RP HPLC分离制备银杏酸α1单体。结果 :银杏酸α1的提取率达 84%以上 ,纯度可达 98%。结论 :该方法简便易行 ,大大降低了工作量。
Objective:To develope a method for the separation and preparation ginkgolic acid α 1. Methods: Ginkgolic acids were extracted by alcohol, and adsorbed by silica gel to remove most of the polar impurities. It was preparated with RP HPLC. Results: The extraction ratio of ginkgolic acid α 1 by this extraction process was above 84%, and the purity of ginkgolic acid α 1 reached 98%. Conclusion: This procedure is simple and relatively effective.
出处
《中成药》
CAS
CSCD
北大核心
2002年第1期54-56,共3页
Chinese Traditional Patent Medicine
