Waugh结构(NH_4)_6[MnMo_9O_(32)]8H_2O的合成与表征

Synthesis and Characterization of Waugh Structural Compound (NH_4)_6[MnMo_9O_(32)]8H_2O

利用三因素三水平正交实验确定了 (NH4 ) 6 [MnMo9O32 ]8H2 O合成的最佳条件 .利用红外、紫外 -可见、差热 -热重和X射线对该化合物进行了表征 .

The optimum experimental conditions were found for synthesizing (NH 4) 6[MnMo 9O 32 ]8H 2O compound by orthogonal method.(NH 4) 6[MnMo 9O 32 ]8H 2O compound was characterized by using Infrared Spectrum, Ultraviolet -visible spectrum, Differential Thermal Analysis(DTA)-Thermal Gravimetry(TG) and X-Ray Diffraction(XRD). The behavior of oxidation-reduction of (NH 4) 6[MnMo 9O 32 ]8H 2O compound was studied by Cyclic Voltammetry(CV).