摘要
用电化学法还原水杨酸制得水杨醛 ,通过正交设计找出最优工艺条件 :电流密度为 1 8A/ dm2 ,p H=6 .0± 0 .2 ,在此条件下合成水杨醛的实际收率可达 6 6 % .
Salicylic acid was reduced to salicylaldehyde electrochemically.The process was optimized by the orthogonalizing method and under the optimum conditions of 18 A/dm 2,pH=6.0± 0.2,the yield 66% of salicylaldehyde could be achieved.
出处
《河北师范大学学报(自然科学版)》
CAS
2002年第1期51-52,56,共3页
Journal of Hebei Normal University:Natural Science
基金
河北省科技厅重点研究和发展计划 ( 992 130 85 D)