摘要
改进和完善苍蓝口服液中盐酸小檗碱含量测定的供试品溶液制备方法。精密量取苍蓝口服液5mL,置25mL容量瓶中,加流动相稀释至刻度,摇匀,过滤,取续滤液作为供试品溶液。结果表明,供试品溶液制备改进后的方法简单高效、准确性高、重现性好,适用于苍蓝口服液中盐酸小檗碱含量检测。
To improve and perfect the preparation method of the sample solution for berberine hydrochloride determination in Canglan oral liquid.Take Precisely 5mL Canglan oral liquid and dilute to volume with mobile phase in a 25mL volumetric flask,shake,filter,and continue to use the filtrate as the sample solution.The established method was simple,accurate and sensitive,which could be applied to the quality control of Canglan oral liquid.
作者
张传津
魏秀丽
陈志强
张娜
陈静
ZHANG Chuanjin;WEI Xiuli;CHEN Zhiqiang;ZHANG Na;CHEN jing(Shandong Veterinary Drug Quality Inspection Institute,Jinan Shangdong 250022,China;Baoding Jizhong pharmaceutical co.LTD,Baoding Hebei 071000,China)
出处
《中兽医医药杂志》
2018年第6期41-44,共4页
Journal of Traditional Chinese Veterinary Medicine
基金
用于家禽保肾、通肾的国家三类新兽药:“苍蓝口服液”,编号:14C1303123002
关键词
苍蓝口服液
盐酸小檗碱
供试品溶液
含量测定
Canglan oral liquid
berberine hydrochloride
preparation method of the sample solution
content measure