摘要
采用改进的Hummers法合成氧化石墨烯(GO),利用原位聚合法合成GO/聚3,4-二氧乙烯噻吩∶聚苯乙烯磺酸(GO/PEDOT∶PSS)复合材料,并使用碘化氢整体还原法生成还原氧化石墨烯(RGO)/PEDOT∶PSS复合材料,同时考察了GO掺杂量对RGO/PEDOT∶PSS复合材料电化学性能的影响。通过X射线衍射仪、拉曼光谱仪、扫描电子显微镜、电化学测试等方法对所制材料进行了表征和性能测试。结果表明:GO与PEDOT∶PSS的质量比为6∶20时合成的RGO/PEDOT∶PSS复合材料具有最佳的电化学性能。
Using a modified Hummers method,graphene oxide(GO)was synthesized.Then GO/PEDOT∶PSS composites were synthesized by in-situ polymerization,and reduced with HI to get RGO/PEDOT∶PSS.The electrochemical performance of RGO/PEDOT∶PSS with different content of GO were analyzed using electrochemical test.RGO/PEDOT∶PSS were characterized by XRD,Raman and SEM.It was found that when the dose proportion of GO and PEDOT∶PSS was 6∶20,the RGO/PEDOT∶PSS had best electrochemical properties.
作者
朱雪乔
杜鹃
袁琪
罗艳
钟毅
Zhu Xueqiao;Du Juan;Yuan Qi;Luo Yan;Zhong Yi(Key Laboratory of Science&Technology of Eco-Textile,Ministry of Education,Donghua University,Shanghai 201620;Wujiang Entry Exit Inspection and Quarantine Bureau, Suzhou 215200)
出处
《化工新型材料》
CAS
CSCD
北大核心
2018年第12期151-155,共5页
New Chemical Materials
