摘要
目的 :研究复方人参注射液的色谱指纹谱测定方法。方法 :以人参皂苷Re为对照品 ,应用HPLC法 ,色谱柱 :ZORBAXSB C18(4 .6× 2 5 0mm ,5 Micro) ,流动相 :乙腈 :水 (梯度洗脱 ) ,柱温 :30°C ,检测波长 :2 0 3nm ,分析时间 :77min ,流速 :1.0mL·min-1。结果 :标示出复方人参注射液 2 7个共有峰。结论 :该方法准确、重复性好 ,为复方人参注射液的指纹图谱质量控制提供了依据。
Objective: To establish the fingerprint chromatogram of Compound Renshen Injection (CRSI). Methods: HPLC with ZORBAX SB-C18[4.6(i.d)×250mm] column was used, the acetonitrile-water (gradient elution) as a mobile phase and detection wavelength at 203nm. Results: Indicating 27 peaks on the HPLC-fingerprint of CRSI. Conclusion: The method is simple and accurate with a good reproducibility and can be used as a quality control method for CRSI.
出处
《中成药》
CAS
CSCD
北大核心
2002年第4期243-245,共3页
Chinese Traditional Patent Medicine
