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亚氨基二乙酸的高效液相色谱测定 被引量:5

HPLC DETERMINATION OF IMINODIACETIC ACID (IDA)
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摘要 利用高效液相色谱 ,采用外标法测定样品中亚氨基二乙酸的含量 ,紫外检测器检测波长为 2 10nm ,色谱柱为SAX强阴离子交换柱 ,用 0 .0 0 5mol·L- 1磷酸二氢钾缓冲液 (pH 2 .5 )为流动相 ,对样品进行分析。其线性相关系数为 0 .9996,标准偏差为 0 .0 35 ,回收率为 98.5 %~ 10 1.5 %。 The determination of IDA by HPLC by external standard method was described. A solution of 0 005mol·L -1 of KH 2PO 4 (pH 2.5) was used as the mobile phase. SAX column was used and the UV detection at 210nm was applied. The correlation coefficient was found to be 0.9996 and the standard deviation was 0.035. Recoveries were found in the range of 98.5%~101.5%.
出处 《理化检验(化学分册)》 CAS CSCD 北大核心 2002年第4期192-193,共2页 Physical Testing and Chemical Analysis(Part B:Chemical Analysis)
关键词 亚氨基二乙酸 高效液相色谱 测定 外标法 紫外检测器 定量分析 HPLC Iminodiacetic acid UV detector External standard method
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参考文献1

  • 1S. G. Chen,K. L. Cheng,Corazon R. Vogt. Ion chromatographic separation of some aminopolycarboxylic acids and inorganic anions[J] 1983,Mikrochimica Acta(5-6):473~481

同被引文献14

  • 1籍秀梅,杨崇,杨军,彭新湘.高效液相色谱法测定植物叶片中乙醇酸及几种酮酸含量[J].分析化学,2005,33(4):527-530. 被引量:9
  • 2刘勇,王玉萍,袁俊秀,彭盘英.亚氨基二乙酸酸化母液的资源化研究[J].南京师大学报(自然科学版),2005,28(3):61-64. 被引量:2
  • 3冯练享,陈均志,任便利.亚氨基二乙酸的生产与应用[J].农药,2006,45(1):12-14. 被引量:14
  • 4徐六兴,许文松,王蓓,栗更新.草甘膦中间体亚氨基二乙酸合成新工艺[J].农药,2006,45(11):751-753. 被引量:10
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