摘要
作者通过实验,探讨了淀粉氧化法制草酸的反应温度及控制,硝硫混酸比例,硝酸投入量,NO_x回收利用,以及母液循环方式等几个方面的最佳选择。研究成果用于生产实践,取得了较好效果。
Reaction temperature and its controlthe mixing ratio of nitric acid to sulfuric acid,amount of HNO_3,the recovery and utilization of NO_x,the recycling of mother liquor.are optimized in the preparation of oxalic acid from starch. Findings in this work have found satisfactory application in commercial production.
关键词
草酸
淀粉氧化法
条件选择
oxalic acid
oxidation of starch
scrutinization of laboratory conditions