摘要
Naphthyl acetate was synthesized in yield of 96.8% using sodium bisulfate as catalyst. The optimum conditions were as follows: β naphthol 3 6 g, acetic anhydride 3 mL, sodium bisulfate 0 5 g , temperature 80 ℃, reaction time 40 min . The method has advantages of cheapness and simplicity , and the catalyst can be easily regenerated.
Naphthyl acetate was synthesized in yield of 96.8% using sodium bisulfate as catalyst. The optimum conditions were as follows: β naphthol 3 6 g, acetic anhydride 3 mL, sodium bisulfate 0 5 g , temperature 80 ℃, reaction time 40 min . The method has advantages of cheapness and simplicity , and the catalyst can be easily regenerated.
出处
《应用化学》
CAS
CSCD
北大核心
2002年第5期509-510,共2页
Chinese Journal of Applied Chemistry
基金
福建省高校重点科技项目基金资助 (JA992 10)
关键词
乙酸β-萘酯
催化酯化
硫酸氢钠
naphthyl acetate,catalytic esterification,sodium bisulfate